erythro-3-(p-hydroxyphenyl)-4-hexane

Base Information

Chemical Name:erythro-3-(p-hydroxyphenyl)-4-hexane
CAS No.:76412-08-3
Molecular Formula:C₂₀H₂₃BrO₂
Molecular Weight:375.305
Hs Code.:

erythro-3-(p-hydroxyphenyl)-4-<p-(bromoacetyl)phenyl>hexane

Synonyms:erythro-3-(p-hydroxyphenyl)-4-hexane

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Chemical Property of erythro-3-(p-hydroxyphenyl)-4-hexane

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Technology Process of erythro-3-(p-hydroxyphenyl)-4-hexane

There total 5 articles about erythro-3-(p-hydroxyphenyl)-4-hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 76412-09-4
erythro-3-(p-hydroxyphenyl)-4-(p-acetylphenyl)hexane

: 76412-08-3
erythro-3-(p-hydroxyphenyl)-4-hexane

Guidance literature:: With copper(ll) bromide; In ethyl acetate; for 9h; Heating;
DOI:10.1021/jm00136a013

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 76412-08-3
erythro-3-(p-hydroxyphenyl)-4-hexane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃, 2.) H₂ / 2.) 5percent Pd/C / 1.) acetone, reflux, 17 h, 2.) ethanol, 37 psi, 35 deg C

2: 90 percent / pyridine / Ambient temperature

3: 65 percent / AlCl₃ / CS₂ / 7 h / Heating

4: 97 percent / 2percent ethanolic KOH / 3 h / Heating

5: 67 percent / cupric bromide / ethyl acetate / 9 h / Heating

With pyridine; potassium hydroxide; aluminium trichloride; hydrogen; potassium carbonate; copper(ll) bromide; palladium on activated charcoal; In carbon disulfide; ethyl acetate;
DOI:10.1021/jm00136a013

Reference yield:

: 3929-22-4,5776-73-8,5776-74-9
deoxyhexestrol

: 76412-08-3
erythro-3-(p-hydroxyphenyl)-4-hexane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / Ambient temperature

2: 65 percent / AlCl₃ / CS₂ / 7 h / Heating

3: 97 percent / 2percent ethanolic KOH / 3 h / Heating

4: 67 percent / cupric bromide / ethyl acetate / 9 h / Heating

With pyridine; potassium hydroxide; aluminium trichloride; copper(ll) bromide; In carbon disulfide; ethyl acetate;
DOI:10.1021/jm00136a013