C₃₅H₄₄O₆

Base Information

Chemical Name:C₃₅H₄₄O₆
CAS No.:236746-21-7
Molecular Formula:C₃₅H₄₄O₆
Molecular Weight:560.731
Hs Code.:

C<sub>35</sub>H<sub>44</sub>O<sub>6</sub>

Synonyms:C₃₅H₄₄O₆

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Chemical Property of C₃₅H₄₄O₆

Chemical Property:

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Technology Process of C₃₅H₄₄O₆

There total 38 articles about C₃₅H₄₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 236746-20-6
C₃₇H₄₈O₇

: 236746-21-7
C₃₅H₄₄O₆

Guidance literature:: With hydrogenchloride; In methanol; at 70 ℃; for 0.75h;
DOI:10.1021/ja990404v

Reference yield:

: 98-88-4
benzoyl chloride

: 236746-21-7
C₃₅H₄₄O₆

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP, pyridine / 5 h / 100 °C

2: aq. HCl / methanol / 0.75 h / 70 °C

With pyridine; hydrogenchloride; dmap; In methanol;
DOI:10.1021/ja990404v

Reference yield:

: 172906-75-1
2-methyl-2-propen-1-yl diazoacetate

: 236746-21-7
C₃₅H₄₄O₆

Guidance literature:: Multi-step reaction with 30 steps

1: 62 percent / <(R,R)-bis2O-)>-C(CH₃)2>*CuOTf / CHCl₃ / Ambient temperature

2: 1.) MeAl / 1.) toluene, from 0 deg C to RT, 30 min, 2.) toluene, RT, 30 min

3: 92 percent / N-methylmorpholine-N-oxide, tetra-n-propylammonium perruthenate, 4 Angstroem sieves / CH₂Cl₂; acetonitrile / 0.5 h / Ambient temperature

4: 1.) potassium hexamethyldisilazide / 1.) toluene, THF, from 0 deg C to RT, 30 min, 2.) toluene, THF, from -78 deg C to 0 deg C, 1 h

5: 1.) t-BuLi / 1.) ether, -78 deg C, 2.) ether

6: Et₃N / -25 °C

7: 24 h / 110 °C

8: aq. HCl

9: 90 percent / tetrahydrofuran / 0 °C

10: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 23 °C

11: 1.) Red-Al, 2.) N-iodosuccinimide / 1.) Et₂O, 23 deg C, 2.) Et₂O, from -78 deg C to 23 deg C

12: 97 percent / imidazole / dimethylformamide

13: Pd(OAc)2, Ph₃P, Ag₂CO₃ / tetrahydrofuran / Heating

14: tetrabutylammonium fluoride / tetrahydrofuran / 23 °C

15: 95 percent / N-methylmorpholin-N-oxide, tetra-n-propylammonium perruthenate

16: 1.) LiBr, Ni(acac)2 / 1.) Et₂O, 0 deg C, 10 min, 2.) Et₂O, RT, 17 h

17: 2-methoxy-1,3-dioxolane, Amberlyst-15 acidic resin / acetonitrile / 12 h / Ambient temperature

18: m-chloroperbenzoic acid, NaHCO₃ / CH₂Cl₂ / 3 h / 0 - 20 °C

19: LiAlH₄ / diethyl ether; tetrahydrofuran / 14 h / Ambient temperature

20: 20 percent aq. HCl / tetrahydrofuran / 12 h / 50 °C

21: N,N-diisopropylethylamine / CH₂Cl₂ / 7 h / Ambient temperature

22: 2.) Et₃N / 1.) toluene, THF, 0 deg C, 10 h, 2.) THF, from 0 deg C to RT

23: 1M aq. HCl / tetrahydrofuran / 0.25 h / Ambient temperature

24: LiAlH₄ / tetrahydrofuran / 0.5 h / -78 °C

25: pyridine, DMAP / CH₂Cl₂ / 2 h / 0 °C

26: 1.) LDA / 1.) hexane, THF, 0 deg C, 15 min, 2.) hexane, THF, 0 deg C, 2 h

27: K₂CO₃, KOH / methanol / 24 h / 140 °C

28: diethyl ether / 0.5 h / 0 °C

29: DMAP, pyridine / 5 h / 100 °C

30: aq. HCl / methanol / 0.75 h / 70 °C

With 2-methoxy-1,3-dioxolane; pyridine; 1H-imidazole; hydrogenchloride; dmap; palladium diacetate; bis(acetylacetonate)nickel(II); potassium hydroxide; N-iodo-succinimide; lithium aluminium tetrahydride; tetrapropylammonium perruthennate; <(R,R)-bis-C(CH3)2>*CuOTf; 4 A molecular sieve; Amberlyst-15 acidic resin; tetrabutyl ammonium fluoride; tert.-butyl lithium; potassium hexamethylsilazane; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; silver carbonate; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja990404v