1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene

Base Information

• Chemical Name: 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene
• CAS No.: 1237706-56-7
• Molecular Formula: C₂₄H₂₈N₂O₂
• Molecular Weight: 376.499

Synonyms:1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene

Chemical Property of 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene

Chemical Property:

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Technology Process of 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene

There total 46 articles about 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H34N2O3 (1362343-46-1) + C33H46N2O3 (1403963-33-6) → Octanal (124-13-0) + 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene (1237706-56-7) + benzaldehyde (100-52-7)

Guidance literature:

In benzene-d6; at 60 ℃; for 2h;

DOI:10.1021/ol302596r

Reference yield:

C31H34N2O3 (1362343-46-1) + C31H33N3O5 (1362343-48-3) → 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene (1237706-56-7) + 4-nitrobenzaldehdye (555-16-8) + benzaldehyde (100-52-7)

Guidance literature:

In benzene-d6; at 60 ℃; for 2h;

DOI:10.1021/ol302596r

Reference yield:

C31H34N2O3 (1362343-46-1) + C31H33BrN2O3 (1403963-31-4) → 1,3-bis-(2,4,6-trimethylphenyl)-4,6-diketo-5,5-dimethylpyrimidin-2-ylidene (1237706-56-7) + benzaldehyde (100-52-7) + 4-bromo-benzaldehyde (1122-91-4)

Guidance literature:

In benzene-d6; at 60 ℃; for 2h;

DOI:10.1021/ol302596r

upstream raw materials:

2-chloro-1,3-dimesityl-5,5-dimethyldihydropyrimidine-4,6(1H,5H)-dione

C₃₁H₃₃N₃O₂

C₃₁H₃₂N₄O₄

C₃₂H₃₅N₃O₃

Downstream raw materials:

2-amino-1,3-dimesityl-5,5-dimethyl-hexahydropyrimidin-4,6-dione

2-oxomethylene-1,3-dimesityl-4,6-diketo-5,5-dimethylpyrimidine

2-((2,6-dimethylphenylimino)methylene)-1,3-dimesityl-4,6-diketo-5,5-dimethylpyrimidine

C₃₀H₄₀N₂O₂Si

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