6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

Base Information

Chemical Name:6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid
CAS No.:1056010-66-2
Molecular Formula:C₁₇H₁₄ClN₃O₄*ClH
Molecular Weight:396.23
Hs Code.:

Synonyms:6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

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Chemical Property of 6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

Chemical Property:

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Technology Process of 6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

There total 2 articles about 6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28443-50-7
2-amino-5-chlorophenol

: 230955-75-6
6-acetoxy-4-chloro-7-methoxyquinazoline

: 1056010-66-2
6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

Guidance literature:: In isopropyl alcohol; at 85 ℃; for 4h;

Reference yield:

: 179688-53-0
7-methoxy-4-oxo-3,4-dihydroquinazolin-6-yl acetate

: 1056010-66-2
6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

Guidance literature:: Multi-step reaction with 2 steps

1: DMF (N,N-dimethyl-formamide) / 5 h / Heating / reflux

2: isopropyl alcohol / 4 h / 85 °C

In DMF (N,N-dimethyl-formamide); isopropyl alcohol;

Reference yield:

: 1056010-66-2
6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid

: 4286-55-9
1-bromo-6-hexanol

: 6-quinazolinol, 4-[[4-chloro-2-[(6-hydroxyhexyl)oxy]phenyl]amino]-7-methoxy-, 6-acetate

Guidance literature:: 6-quinazolinol,4-[(4-chloro-2-hydroxyphenyl)amino]-7-methoxy-,6-acetate monohydrochloric acid; With sodium hydride; In ISOPROPYLAMIDE; at 20 ℃; for 0.5h;

1-bromo-6-hexanol; In ISOPROPYLAMIDE; at 20 ℃;