2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

Base Information

Chemical Name:2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)
CAS No.:1443300-32-0
Molecular Formula:C₃₃H₅₀N₂O₁₈P₂
Molecular Weight:824.71
Hs Code.:

Synonyms:2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

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Chemical Property of 2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

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Technology Process of 2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

There total 13 articles about 2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1443300-62-6
2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(3-(3-((bis(benzyloxy)phosphoryl)oxy)propoxy)-2,2-dimethylpropanoate)

: 1443300-32-0
2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 40 ℃;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1443300-32-0
2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

Guidance literature:: Multi-step reaction with 7 steps

1: sodium acetate; sodium iodide / water / 3 h / 90 °C

2: water; sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 40 °C

3: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 1 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 60 °C

5: sodium ethanolate / ethanol / 1.5 h / 85 °C

6: triethylamine / dichloromethane / 16 h / 0 - 20 °C

7: hydrogen; palladium 10% on activated carbon / methanol / 40 °C

With palladium 10% on activated carbon; water; hydrogen; sodium ethanolate; sodium acetate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 98269-30-8
diethyl 2,2’-((4-methoxyphenyl)azanediyl)diacetate

: 1443300-32-0
2-(dimethylcarbamoyl)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl bis(2,2-dimethyl-3-(3-(phosphonooxy)propoxy)propanoate)

Guidance literature:: Multi-step reaction with 7 steps

1: sodium ethanolate / ethanol / 1 h / 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

3: water; sodium hydroxide / tetrahydrofuran; ethanol / 16 h / 50 °C

4: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

5: hydrogen; palladium 10% on activated carbon / ethanol / 1.5 h / 20 °C

6: triethylamine / dichloromethane / 16 h / 0 - 20 °C

7: hydrogen; palladium 10% on activated carbon / methanol / 40 °C

With palladium 10% on activated carbon; water; hydrogen; sodium ethanolate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;