(E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Base Information

Chemical Name:(E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid
CAS No.:853794-93-1
Molecular Formula:C₂₁H₂₂O₈
Molecular Weight:402.401
Hs Code.:

Synonyms:(E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Suppliers and Price of (E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

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Technology Process of (E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

There total 2 articles about (E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 108-24-7
acetic anhydride

: 121-33-5,8014-42-4
vanillin

: 853794-93-1
(E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Guidance literature:: 3,4,5-trimethoxyphenyl acetic acid; acetic anhydride; vanillin; With triethylamine; at 140 ℃; for 24h;

With hydrogenchloride; In water; at 20 ℃;
DOI:10.1016/j.bmc.2011.06.017

Reference yield:

: 881-68-5
vanillin acetate

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 853794-93-1
(E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Guidance literature:: With acetic anhydride; triethylamine; at 140 ℃;
DOI:10.1016/j.bmc.2019.06.007

Reference yield: 91.0%

: 853794-93-1
(E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

: (1-(3-fluorophenyl)-9H-pyrido[3,4-b]indol-3-yl)methanamine

: (E)-4-(3-(((1-(3-fluorophenyl)-9H-pyrido[3,4-b]indol-3-yl)methyl)amino)-3-oxo-2-(3,4,5-trimethoxyphenyl)prop-1-en-1-yl)-2-methoxyphenyl acetate

Guidance literature:: (E)-3-(4'-acetoxy-3'-methoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

(1-(3-fluorophenyl)-9H-pyrido[3,4-b]indol-3-yl)methanamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2019.06.007