{2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

Base Information

Chemical Name:{2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide
CAS No.:1423783-89-4
Molecular Formula:C₂₄H₂₈NO₅*I
Molecular Weight:537.395
Hs Code.:

Synonyms:{2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

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Technology Process of {2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

There total 4 articles about {2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1-(3-((dimethylamino)methyl)-4-hydroxyphenyl)-7-(4-hydroxy-3-methoxyphenyl)hepta-1,6-diene-3,5-dione

: 74-88-4
methyl iodide

: 1423783-89-4
{2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

Guidance literature:: In acetonitrile; at 20 ℃;
DOI:10.1016/j.bmcl.2012.12.098

Reference yield:

: 6-(3-((dimethylamino)methyl)-4-hydroxyphenyl)hex-5-ene-2,4-dione

: 1423783-89-4
{2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diboron trioxide / ethyl acetate / 0.5 h / 40 °C

1.2: 0.5 h / 40 °C

1.3: 40 °C

2.1: acetonitrile / 20 °C

With diboron trioxide; In ethyl acetate; acetonitrile;
DOI:10.1016/j.bmcl.2012.12.098

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1423783-89-4
{2-hydroxy-5-[7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dienyl]phenyl}-N,N,N-trimethylmethanaminium iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; methanol / 50 °C

2.1: diboron trioxide / ethyl acetate / 0.5 h / 40 °C

2.2: 40 °C

3.1: diboron trioxide / ethyl acetate / 0.5 h / 40 °C

3.2: 0.5 h / 40 °C

3.3: 40 °C

4.1: acetonitrile / 20 °C

With diboron trioxide; In methanol; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmcl.2012.12.098