t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

Base Information

Chemical Name:t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate
CAS No.:1193988-66-7
Molecular Formula:C₂₅H₃₂N₂O₅
Molecular Weight:440.539
Hs Code.:

Synonyms:t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

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Chemical Property of t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

Chemical Property:

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Technology Process of t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

There total 1 articles about t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100955-81-5
(4-(benzyloxy)-3-methoxyphenyl)methanamine hydrochloride

: 140148-70-5
(S)-1-N-boc-β-proline

: 1193988-66-7
t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: 1193988-66-7
t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

: 1194062-14-0
(S)-N-(4-benzyloxy-3-methoxybenzyl)-3-pyrrolidinecarboxamide

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 6h;

Reference yield:

: 1193988-66-7
t-butyl (S)-3-(4-benzyloxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

: 1193988-18-9
4,4-dimethylcyclohexyl (S)-3-(4-hydroxy-3-methoxybenzylcarbamoyl)-pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / ethyl acetate / 6 h

2.1: acetonitrile / 1 h / 45 °C

2.2: 1 h / 80 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 1 h / 20 °C

With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In ethanol; ethyl acetate; acetonitrile;