4,4'-dihexylbenzil

Base Information

Chemical Name:4,4'-dihexylbenzil
CAS No.:869081-44-7
Molecular Formula:C₂₆H₃₄O₂
Molecular Weight:378.555
Hs Code.:

Synonyms:4,4'-dihexylbenzil

Suppliers and Price of 4,4'-dihexylbenzil

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 4,4'-dihexylbenzil

Chemical Property:

Purity/Quality:: HPLC≥98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-dihexylbenzil

There total 6 articles about 4,4'-dihexylbenzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 23703-22-2
1-bromo-4-n-hexylbenzene

: 59417-06-0
1,4-dimethyl-2,3-dioxopiperazine

: 869081-44-7
4,4'-dihexylbenzil

Guidance literature:: 1-bromo-4-n-hexylbenzene; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h;

1,4-dimethyl-2,3-dioxopiperazine; In tetrahydrofuran; cyclohexane; at -40 - 20 ℃; for 15h;

With hydrogenchloride; In tetrahydrofuran; cyclohexane; water;

Reference yield:

: 111-25-1
1-bromo-hexane

: 869081-44-7
4,4'-dihexylbenzil

Guidance literature:: Multi-step reaction with 4 steps

1.1: Mg / tetrahydrofuran

1.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran

2.1: Br₂; Fe; I₂

3.1: Mg / tetrahydrofuran

3.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran

4.1: SeO₂; 90 percent aq. AcOH; H₂SO₄

With selenium(IV) oxide; sulfuric acid; bromine; iodine; iron; magnesium; acetic acid; In tetrahydrofuran; 1.2: Tamao-Kumada reaction / 3.2: Tamao-Kumada reaction;
DOI:10.1039/b007135h

Reference yield:

: 1077-16-3
hexylbenzene

: 869081-44-7
4,4'-dihexylbenzil

Guidance literature:: Multi-step reaction with 3 steps

1.1: Br₂; Fe; I₂

2.1: Mg / tetrahydrofuran

2.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran

3.1: SeO₂; 90 percent aq. AcOH; H₂SO₄

With selenium(IV) oxide; sulfuric acid; bromine; iodine; iron; magnesium; acetic acid; In tetrahydrofuran; 2.2: Tamao-Kumada reaction;
DOI:10.1039/b007135h