5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ²-1,2,4-oxadiazoline

Base Information

• Chemical Name: 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ²-1,2,4-oxadiazoline
• CAS No.: 80650-34-6
• Molecular Formula: C₂₇H₂₃N₃O₄
• Molecular Weight: 453.497

Synonyms:5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ²-1,2,4-oxadiazoline

Chemical Property of 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ²-1,2,4-oxadiazoline

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ²-1,2,4-oxadiazoline

There total 3 articles about 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ²-1,2,4-oxadiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-(m-methoxy-p-hydroxybenzalamino)-3-methyl-5-styrylisoxazole (80650-27-7) + benzohydroximoyl chloride (698-16-8) → 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ2-1,2,4-oxadiazoline (80650-34-6)

Guidance literature:

With triethylamine; In chloroform; at 0 ℃; for 4.25h;

Reference yield:

4-amino-3-methyl-5-styryl isoxazole (53558-01-3) → 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ2-1,2,4-oxadiazoline (80650-34-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / methanol / Heating

2: 60 percent / Et₃N / CHCl₃ / 4.25 h / 0 °C

With triethylamine; In methanol; chloroform;

Reference yield:

vanillin (121-33-5,8014-42-4) → 5-(p-hydroxy-m-methoxyphenyl)-4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-Δ2-1,2,4-oxadiazoline (80650-34-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / methanol / Heating

2: 60 percent / Et₃N / CHCl₃ / 4.25 h / 0 °C

With triethylamine; In methanol; chloroform;

upstream raw materials:

4-(m-methoxy-p-hydroxybenzalamino)-3-methyl-5-styrylisoxazole

benzohydroximoyl chloride

4-amino-3-methyl-5-styryl isoxazole

vanillin

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