3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Base Information

Chemical Name:3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose
CAS No.:280574-37-0
Molecular Formula:C₃₉H₅₀O₁₂
Molecular Weight:710.819
Hs Code.:

Synonyms:3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

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Chemical Property of 3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

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Technology Process of 3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

There total 5 articles about 3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 280574-35-8
[(2S,3R,4S,5R,6R)-4,5-Bis-(4-methoxy-benzyloxy)-6-(4-methoxy-benzyloxymethyl)-2-phenylselanyl-tetrahydro-pyran-3-yloxy]-((3aR,5S,6aR)-2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-dimethyl-silane

: 1-deoxy-3,4,6-tri-O-p-methoxybenzyl-D-glucopyranose

: 3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-gulo-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

: 280574-37-0
3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Guidance literature:: [(2S,3R,4S,5R,6R)-4,5-Bis-(4-methoxy-benzyloxy)-6-(4-methoxy-benzyloxymethyl)-2-phenylselanyl-tetrahydro-pyran-3-yloxy]-((3aR,5S,6aR)-2,2-dimethyl-6-methylene-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-dimethyl-silane; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃;

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)00171-4

Reference yield:

: C₄₁H₅₄O₁₂Si

: 280574-37-0
3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Guidance literature:: With tetrabutyl ammonium fluoride;
DOI:10.1081/NCN-100002320

Reference yield:

: 64775-10-6
((3aR,5S,6aR)-2,2-dimethyl-6-methylene-tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 280574-37-0
3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: BuLi

2: Bu₃SnH; AIBN

3: TBAF

With n-butyllithium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride;
DOI:10.1081/NCN-100002320