5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Base Information

Chemical Name:5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose
CAS No.:289044-96-8
Molecular Formula:C₅₃H₆₂O₁₂
Molecular Weight:891.068
Hs Code.:

5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Synonyms:5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

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Chemical Property of 5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

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Technology Process of 5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

There total 1 articles about 5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 100-39-0
benzyl bromide

: 280574-37-0
3-deoxy-3-(4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

: 289044-96-8
5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo0001333

Reference yield:

: 289044-96-8
5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose

: (2R,3S,4S,5R,6R)-5-Benzyloxy-6-((2S,3S,4R)-2-benzyloxymethyl-4,5-dihydroxy-tetrahydro-furan-3-ylmethyl)-2-hydroxymethyl-tetrahydro-pyran-3,4-diol

Guidance literature:: 5-O-benzyl-3-deoxy-3-(3-O-benzyl-4,5,7-tri-O-p-methoxybenzyl-2,6-anhydro-1-deoxy-D-glycero-D-ido-heptitol-1-yl)-1,2-O-(1-methylethylidene)-α-D-ribo-pentofuranose; With trifluoroacetic acid; In water; at 20 ℃; for 3h;

With sodium methylate; In methanol; at 20 ℃; for 0.5h; Further stages.;
DOI:10.1021/jo0001333