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C29H41NO6Si

Base Information
  • Chemical Name:C29H41NO6Si
  • CAS No.:1265173-09-8
  • Molecular Formula:C29H41NO6Si
  • Molecular Weight:527.733
  • Hs Code.:
C<sub>29</sub>H<sub>41</sub>NO<sub>6</sub>Si

Synonyms:C29H41NO6Si

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Chemical Property of C29H41NO6Si
Chemical Property:
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Technology Process of C29H41NO6Si

There total 16 articles about C29H41NO6Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With potassium carbonate; In tetrahydrofuran; water; at 0 ℃; for 3h;
DOI:10.1002/asia.201000602
Guidance literature:
Multi-step reaction with 11 steps
1.1: acetic anhydride; dimethyl sulfoxide / 2 h / 50 °C
2.1: toluene / 4 h / -40 °C
3.1: magnesium / methanol / 2 h / 20 °C
4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C
5.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C
5.2: 0 - 20 °C
6.1: pyridine / dichloromethane / 2 h / 0 °C
7.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C
8.1: dichloromethane / 1 h / 0 °C
9.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C
10.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C
11.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C
With pyridine; sulfur trioxide pyridine complex; acetic anhydride; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; toluene; mineral oil; 4.1: Swern oxidation / 5.2: Horner-Wadsworth-Emmons olefination / 9.1: Overman rearrangement;
DOI:10.1002/asia.201000602
Guidance literature:
Multi-step reaction with 10 steps
1.1: toluene / 4 h / -40 °C
2.1: magnesium / methanol / 2 h / 20 °C
3.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C
4.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C
4.2: 0 - 20 °C
5.1: pyridine / dichloromethane / 2 h / 0 °C
6.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C
7.1: dichloromethane / 1 h / 0 °C
8.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C
9.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C
10.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C
With pyridine; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; toluene; mineral oil; 3.1: Swern oxidation / 4.2: Horner-Wadsworth-Emmons olefination / 8.1: Overman rearrangement;
DOI:10.1002/asia.201000602
upstream raw materials:

C22H28O7S

C22H26O7S

C23H30O7S

C16H24O5

Downstream raw materials:

NPI-2077

C25H31NO6

C26H33NO6

C25H27NO6

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