C₃₆H₅₅NO

Base Information

• Chemical Name: C₃₆H₅₅NO
• CAS No.: 1620005-01-7
• Molecular Formula: C₃₆H₅₅NO
• Molecular Weight: 517.839
• Mol file: 1620005-01-7.mol

Synonyms:C₃₆H₅₅NO

Chemical Property of C₃₆H₅₅NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₆H₅₅NO

There total 2 articles about C₃₆H₅₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

lupenone (1617-70-5) + N-phenyl hydroxylamine hydrochloride (22755-09-5) → C36H55NO (1620005-01-7)

Guidance literature:

With pyridine; for 3h; Reflux; Inert atmosphere;

DOI:10.1016/j.bmcl.2014.05.032

Reference yield:

lupenol (545-47-1) → C36H55NO (1620005-01-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; Jones reagent / chloroform / 0.17 h / 20 °C / Cooling with ice

2: pyridine / 3 h / Reflux; Inert atmosphere

With pyridine; Jones reagent; acetic acid; In chloroform; 1: |Jones Oxidation;

DOI:10.1016/j.bmcl.2014.05.032

upstream raw materials:

lupenone

N-phenyl hydroxylamine hydrochloride

lupenol

Refernces