3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde

Base Information

Chemical Name:3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde
CAS No.:866206-35-1
Molecular Formula:C₄₇H₃₀N₄OZn
Molecular Weight:732.171
Hs Code.:

Synonyms:3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde

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Chemical Property of 3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde

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Technology Process of 3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde

There total 1 articles about 3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3-(5',10',15',20'-tetraphenylporphyrin-2'-yl)allyl aldehyde

: 5970-45-6
zinc(II) acetate dihydrate

: 866206-35-1
3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde

Guidance literature:: In methanol; chloroform; under N2 or Ar; shielded from ambient light; soln. of Zn(OAc)2*2H2O in MeOH added to soln. of porphyrin in CHCl3 with stirring at room temp.; reaction completed after 10 min (monitoring by TLC); pptn. from MeOH;
DOI:10.1021/jp052877w

Reference yield: 84.0%

: 866206-35-1
3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))allyl aldehyde

: 372-09-8
cyanoacetic acid

: 866269-30-9,911384-95-7
2-cyano-5-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))penta-2,4-dienoic acid

Guidance literature:: With piperidine; In methanol; shielded from ambient light; soln. of Zn porphyrin complex, cyanoacetic acid and piperidine in MeOH refluxed for 50 min under N2; cooled; CH2Cl2 and H2O added; shaken; aq. layer adjusted with 2 M H3PO4 to pH 2; org. layer sepd.; CH2Cl2 removed by azeotrope distn. with CH3CNin vac.; pptn. with H2O; filtered; solid dissolved in CHCl3 and little THF; filtered; pptn. with hexane;
DOI:10.1021/jp052877w