Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

Base Information

Chemical Name:Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester
CAS No.:130312-98-0
Molecular Formula:C₁₆H₁₈O₅
Molecular Weight:290.316
Hs Code.:

Synonyms:Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

Chemical Property:

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Technology Process of Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

There total 1 articles about Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41878-37-9
1β-benzoyloxy-7aβ-methyl-5,6,7,7a-tetrahydroindan-5-one

: 130312-98-0
Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

Guidance literature:: With ozone; In methanol; at -78 ℃;
DOI:10.1016/S0040-4039(00)94472-1

Reference yield:

: 130312-98-0
Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

: 145345-95-5
Benzoic acid (1S,2R)-2-(3-hydroxy-propyl)-2-methyl-3-oxo-cyclopentyl ester

Guidance literature:: With borane-THF; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(00)94472-1

Reference yield:

: 130312-98-0
Benzoic acid (1S,2R)-2-(2-carboxy-ethyl)-2-methyl-3-oxo-cyclopentyl ester

: 130313-05-2
methyl 17β-benzoyloxy-3-isopropyl-1,7-dioxo-5β-androsta-2,8(14)-dien-19-oate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) BH₃*THF, 2.) pyridinium chlorochromate (PCC) / 1.) THF, 0 deg C, 2 h, 2.) CH₂Cl₂, room temperature, 3 h

2: 73 percent / benzene / 48 h / Heating

3: 1.) Zn, I₂ / 1.) THF, reflux, 1 h, 2.) THF, 0 deg C, 90 min

4: 58 percent / MnO₂ / ethyl acetate / 8 h / Ambient temperature

5: 1.) Cs₂CO₃, 2.) CF₃CO₂H / 1.) CHCl₃, room temperature, 6 h, 2.) benzene, reflux, 5 h

6: 77 percent / p-toluenesulfonic acid / benzene / 16 h / Heating

With manganese(IV) oxide; borane-THF; iodine; caesium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; trifluoroacetic acid; zinc; In ethyl acetate; benzene;
DOI:10.1139/v92-243