C₃₆H₅₂NO₄ISi

Base Information

Chemical Name:C₃₆H₅₂NO₄ISi
CAS No.:944800-40-2
Molecular Formula:C₃₆H₅₂INO₄Si
Molecular Weight:717.803
Hs Code.:

C<sub>36</sub>H<sub>52</sub>NO<sub>4</sub>ISi

Synonyms:C₃₆H₅₂NO₄ISi

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Chemical Property of C₃₆H₅₂NO₄ISi

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Technology Process of C₃₆H₅₂NO₄ISi

There total 9 articles about C₃₆H₅₂NO₄ISi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 944800-39-9
C₃₀H₃₈NO₄I

: 18162-48-6
tert-butyldimethylsilyl chloride

: 944800-40-2
C₃₆H₅₂NO₄ISi

Guidance literature:: With 1H-imidazole; In dichloromethane;
DOI:10.1016/j.tet.2007.02.106

Reference yield:

: 944800-23-1
C₂₂H₂₂O₂

: 944800-40-2
C₃₆H₅₂NO₄ISi

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylsulfoxide

1.2: 78 percent / dimethylsulfoxide / 14 h

2.1: 84 percent / Et₂AlCl / CH₂Cl₂; toluene / -20 °C

3.1: 73 percent / BCl₃ / CH₂Cl₂; methanol / -78 °C

4.1: 82 percent / imidazole; PPh₃; I₂ / CH₂Cl₂ / -40 - 20 °C

5.1: 93 percent / imidazole / CH₂Cl₂

With 1H-imidazole; iodine; diethylaluminium chloride; boron trichloride; sodium hydride; triphenylphosphine; In methanol; dichloromethane; dimethyl sulfoxide; toluene; 2.1: Diels-Alder cycloaddition;
DOI:10.1016/j.tet.2007.02.106

Reference yield:

: 944800-26-4
C₃₀H₃₉NO₅

: 944800-40-2
C₃₆H₅₂NO₄ISi

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / imidazole; PPh₃; I₂ / CH₂Cl₂ / -40 - 20 °C

2: 93 percent / imidazole / CH₂Cl₂

With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane;
DOI:10.1016/j.tet.2007.02.106