N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide

Base Information

Chemical Name:N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide
CAS No.:1381808-52-1
Molecular Formula:C₂₄H₃₃NO₂S
Molecular Weight:399.598
Hs Code.:

Synonyms:N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide

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Technology Process of N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide

There total 1 articles about N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 38387-24-5
(3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methanol

: 10285-80-0
N-tosyl-3-butenylamine

: 1381808-52-1
N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/om3004288

Reference yield:

: 201230-82-2
carbon monoxide

: 1381808-52-1
N-(but-3-enyl)-N-((3-(cyclohexylidenemethylene)-2,2-dimethylcyclopropyl)methyl)-4-tolylsulfonamide

: 7-cyclohexylidene-8-(propan-2-ylidene)-2-tosyloctahydroisoquinolin-6(7H)-one

: 7-cyclohexylidene-8-(propan-2-ylidene)-2-tosyloctahydroisoquinolin-6(7H)-one

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; In 1,2-dichloro-ethane; at 80 ℃; for 5h; under 760.051 Torr; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/om3004288