Technology Process of C14H12O3
There total 3 articles about C14H12O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine; palladium dichloride;
at 120 ℃;
for 3h;
under 7600.51 Torr;
Autoclave;
DOI:10.1055/s-0033-1339309
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus tribromide
2: sodium chlorite; dihydrogen peroxide
3: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / Autoclave
With
sodium chlorite; 1,3-bis-(diphenylphosphino)propane; dihydrogen peroxide; phosphorus tribromide; acetic acid; triethylamine; palladium dichloride;
1: |Vilsmeier-Haack Formylation;
DOI:10.1055/s-0033-1339309
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium chlorite; dihydrogen peroxide
2: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / Autoclave
With
sodium chlorite; 1,3-bis-(diphenylphosphino)propane; dihydrogen peroxide; acetic acid; triethylamine; palladium dichloride;
DOI:10.1055/s-0033-1339309