(1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

Base Information

Chemical Name:(1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane
CAS No.:195059-45-1
Molecular Formula:C₂₁H₂₈N₂O₃
Molecular Weight:356.465
Hs Code.:

(1S,2S)-N<sup>1</sup>-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

Synonyms:(1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

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Chemical Property of (1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

Chemical Property:

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Technology Process of (1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

There total 3 articles about (1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-58-3
phenylmagnesium bromide

: 162740-15-0
(Z)-N-<(2S)-2-(tert-butoxycarbonylamino)propylidene> benzylamine N-oxide

: 195059-45-1
(1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

Guidance literature:: In tetrahydrofuran; at -40 ℃; for 4h;
DOI:10.1016/S0957-4166(97)00250-4

Reference yield:

: 79069-50-4
Boc-Ala-H

: 195059-45-1
(1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / MgSO₄ / CH₂Cl₂ / 4 h / 20 °C

2: 85 percent / tetrahydrofuran / 4 h / -40 °C

With magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(97)00250-4

Reference yield:

: 622-30-0
N-benzyl hydroxylalmine

: 195059-45-1
(1S,2S)-N¹-benzyl-2-(tert-butoxycarbonylamino)-1-(hydroxyamino)-1-phenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / MgSO₄ / CH₂Cl₂ / 4 h / 20 °C

2: 85 percent / tetrahydrofuran / 4 h / -40 °C

With magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(97)00250-4