ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

Base Information

Chemical Name:ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate
CAS No.:168909-65-7
Molecular Formula:C₁₇H₂₆ClO₅P
Molecular Weight:376.817
Hs Code.:

Synonyms:ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

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Chemical Property of ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

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Technology Process of ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

There total 3 articles about ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1026966-90-4
C₉H₂₃O₂PSi

: 168909-99-7
ethyl 1-(4-chlorophenyl)oxirane-1-carboxylate

: 168909-65-7
ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

Guidance literature:: With zinc(II) chloride; In tetrahydrofuran; for 6h; Heating;
DOI:10.1021/jm00017a016

Reference yield:

: 21661-52-9
ethyl butylphosphinate

: 168909-65-7
ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 24 h / Ambient temperature

2: 62 percent / ZnCl₂ / tetrahydrofuran / 6 h / Heating

With triethylamine; zinc(II) chloride; In tetrahydrofuran;
DOI:10.1021/jm00017a016

Reference yield:

: 101492-44-8
ethyl 2-(4-chlorophenyl)acrylate

: 168909-65-7
ethyl (1-carbethoxy-2-(4-chlorophenyl)-2-hydroxyethyl)n-butylphosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / m-chloroperbenzoic acid / CHCl₃ / 24 h / Heating

2: 62 percent / ZnCl₂ / tetrahydrofuran / 6 h / Heating

With 3-chloro-benzenecarboperoxoic acid; zinc(II) chloride; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00017a016