methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

Base Information

Chemical Name:methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate
CAS No.:236751-38-5
Molecular Formula:C₁₂H₁₃F₃O₇S
Molecular Weight:358.292
Hs Code.:

Synonyms:methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

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Chemical Property of methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

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Technology Process of methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

There total 4 articles about methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1007852-69-8
methyl 2-hydroxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

: 107-30-2
chloromethyl methyl ether

: 236751-38-5
methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 5.5h;
DOI:10.1002/chem.200700863

Reference yield:

: 22375-05-9
methyl 4-benzyloxy-2-hydroxy-6-methylbenzoate

: 236751-38-5
methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: (i-Pr)2NEt / CH₂Cl₂ / 4 h / 40 °C

2: H₂ / Pd(OH)2 / ethyl acetate / 24 h

3: (i-Pr)2NEt / CH₂Cl₂ / 0.5 h / -78 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In dichloromethane; ethyl acetate; 1: Etherification / 2: Hydrogenolysis / 3: Etherification;
DOI:10.1002/(SICI)1521-3773(19990503)38:9<1229::AID-ANIE1229>3.0.CO;2-B

Reference yield:

: 4-benzyloxy-2-methoxymethoxy-6-methyl-benzoic acid methyl ester

: 236751-38-5
methyl 2-methoxymethoxy-6-methyl-4-(trifluoromethylsulfonyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd(OH)2 / ethyl acetate / 24 h

2: (i-Pr)2NEt / CH₂Cl₂ / 0.5 h / -78 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In dichloromethane; ethyl acetate; 1: Hydrogenolysis / 2: Etherification;
DOI:10.1002/(SICI)1521-3773(19990503)38:9<1229::AID-ANIE1229>3.0.CO;2-B