(R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt

Base Information

• Chemical Name: (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt
• CAS No.: 1159502-39-2
• Molecular Formula: C₁₂H₁₅NO₅*C₁₂H₂₃N
• Molecular Weight: 434.576
• Mol file: 1159502-39-2.mol

Synonyms:(R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt

Chemical Property of (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt

There total 3 articles about (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[(phenylmethoxy)carbonyl]-D-homoserine (41088-85-1) + N-cyclohexyl-cyclohexanamine (101-83-7) → (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt (1159502-39-2)

Guidance literature:

In ethanol;

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt (1159502-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / 1,4-dioxane / 20 °C / Cooling with ice

2: ethanol

With sodium hydroxide; In 1,4-dioxane; ethanol;

Reference yield:

→ (R)-2-benzyloxycarbonylamino-4-hydroxybutyric acid, dicyclohexylamine salt (1159502-39-2)

Guidance literature:

upstream raw materials:

N-[(phenylmethoxy)carbonyl]-D-homoserine

N-cyclohexyl-cyclohexanamine

benzyl chloroformate

Downstream raw materials:

(R)-methyl 2-(((benzyloxy)carbonyl)amino)-4-hydroxybutanoate

4-[(R)-2-benzyloxycarbonylamino-4-(diethoxy-phosphoryl)-butyryl]-piperazine-1-carboxylic acid ethyl ester

(R)-2-benzyloxycarbonylamino-4-(diethoxy-phosphoryl)-butyric acid methyl ester

(R)-2-benzyloxycarbonylamino-4-(diethoxy-phosphoryl)-butyric acid