Technology Process of C14H21N3O
There total 4 articles about C14H21N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(4-azidobutyl)triphenyl phosphonium bromide;
With
potassium hexamethylsilazane;
In
tetrahydrofuran; dichloromethane;
at -78 ℃;
for 0.5h;
C10H14O2;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 2.16667h;
DOI:10.1002/adsc.201200071
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 5 h / -78 - 23 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 23 °C / Cooling
2.2: 10 h / 0 °C
2.3: 1 h / 23 °C
3.1: ozone; solvent red 19 / dichloromethane / -78 - 20 °C
3.2: -78 - 20 °C
4.1: potassium hexamethylsilazane / tetrahydrofuran; dichloromethane / 0.5 h / -78 °C
4.2: 2.17 h / -78 - 20 °C
With
lithium aluminium tetrahydride; potassium hexamethylsilazane; ozone; solvent red 19; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1002/adsc.201200071
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ozone; solvent red 19 / dichloromethane / -78 - 20 °C
1.2: -78 - 20 °C
2.1: potassium hexamethylsilazane / tetrahydrofuran; dichloromethane / 0.5 h / -78 °C
2.2: 2.17 h / -78 - 20 °C
With
potassium hexamethylsilazane; ozone; solvent red 19;
In
tetrahydrofuran; dichloromethane;
2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1002/adsc.201200071
