methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

Base Information

Chemical Name:methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside
CAS No.:68880-94-4
Molecular Formula:C₂₈H₃₀O₃
Molecular Weight:414.544
Hs Code.:

Synonyms:methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

Chemical Property:

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Technology Process of methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

There total 6 articles about methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 68880-93-3,90289-88-6
methyl 2,3-dideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranosid-4-ulose

: 1779-49-3
Methyltriphenylphosphonium bromide

: 68880-94-4
methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

Guidance literature:: With n-butyllithium; In diethyl ether; for 28h; Heating;
DOI:10.1139/v82-050

Reference yield:

: 76-83-5
trityl chloride

: 68880-94-4
methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / pyridine / 72 h / Ambient temperature

2: 81 percent / CrO₃ / pyridine; CH₂Cl₂ / 18 h / Ambient temperature

3: 82 percent / n-butyllithium / diethyl ether / 28 h / Heating

With chromium(VI) oxide; n-butyllithium; In pyridine; diethyl ether; dichloromethane;
DOI:10.1139/v82-050

Reference yield:

: 68880-91-1
methyl 2,3-dideoxy-2-C-methyl-α-D-arabino-hexopyranoside

: 68880-94-4
methyl 2,3,4-trideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / pyridine / 72 h / Ambient temperature

2: 81 percent / CrO₃ / pyridine; CH₂Cl₂ / 18 h / Ambient temperature

3: 82 percent / n-butyllithium / diethyl ether / 28 h / Heating

With chromium(VI) oxide; n-butyllithium; In pyridine; diethyl ether; dichloromethane;
DOI:10.1139/v82-050