2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

Base Information

Chemical Name:2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid
CAS No.:170029-59-1
Molecular Formula:C₃₂H₄₆N₂O₈
Molecular Weight:586.726
Hs Code.:

Synonyms:2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

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Chemical Property of 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

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Technology Process of 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

There total 5 articles about 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 170029-58-0
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid

: 170029-59-1
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

Guidance literature:: With nitric acid; acetic acid; for 0.5h; Ambient temperature;
DOI:10.1002/prac.19953370186

Reference yield:

: 1568-70-3
4-methoxy-2-nitrophenol

: 170029-59-1
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / dioxane

2: dioxane / 0.25 h / Heating

3: 84 percent / NaOH, Tetrabutylammoniumiodid / toluene / 0.25 h / 40 - 50 °C

4: 85 percent / 65percent aq. HNO₃, AcOH / 0.5 h / Ambient temperature

With sodium hydroxide; hydrogen; nitric acid; tetra-(n-butyl)ammonium iodide; acetic acid; palladium on activated charcoal; In 1,4-dioxane; toluene;
DOI:10.1002/prac.19953370186

Reference yield:

: 89-39-4
1,4-dimethoxy-2-nitrobenzene

: 170029-59-1
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / LiI, quinoline / 0.25 h / 160 - 170 °C

2: H₂ / 10percent Pd/C / dioxane

3: dioxane / 0.25 h / Heating

4: 84 percent / NaOH, Tetrabutylammoniumiodid / toluene / 0.25 h / 40 - 50 °C

5: 85 percent / 65percent aq. HNO₃, AcOH / 0.5 h / Ambient temperature

With quinoline; sodium hydroxide; hydrogen; nitric acid; tetra-(n-butyl)ammonium iodide; acetic acid; lithium iodide; palladium on activated charcoal; In 1,4-dioxane; toluene;
DOI:10.1002/prac.19953370186