4-n-dodecyloxybenzaldehyde acetal

Base Information

• Chemical Name: 4-n-dodecyloxybenzaldehyde acetal
• CAS No.: 1252583-31-5
• Molecular Formula: C₂₂H₃₆O₄
• Molecular Weight: 364.525
• Mol file: 1252583-31-5.mol

Synonyms:4-n-dodecyloxybenzaldehyde acetal

Chemical Property of 4-n-dodecyloxybenzaldehyde acetal

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-n-dodecyloxybenzaldehyde acetal

There total 1 articles about 4-n-dodecyloxybenzaldehyde acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-dodecylbromide (143-15-7) → 4-n-dodecyloxybenzaldehyde acetal (1252583-31-5)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 14 h / Reflux

2: toluene-4-sulfonic acid / toluene / 14 h / Reflux

With potassium carbonate; toluene-4-sulfonic acid; In acetone; toluene;

DOI:10.1039/c2jm34817a

Reference yield:

4-n-dodecyloxybenzaldehyde acetal (1252583-31-5) + Methacryloyl chloride (920-46-7,26937-45-1) → DBAM (1252583-32-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Cooling with ice;

DOI:10.1039/c0cc01857k

Reference yield:

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 4-n-dodecyloxybenzaldehyde acetal (1252583-31-5) → 2,4-dichloro-dodecyloxybenzalacetal-1,3,5-triazine

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In toluene; for 18h; Inert atmosphere; Reflux;

DOI:10.1002/smll.201503121

upstream raw materials:

1-dodecylbromide

Downstream raw materials:

DBAM