1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide

Base Information

• Chemical Name: 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide
• CAS No.: 134172-74-0
• Molecular Formula: C₃₆H₃₉N₄O₄*I
• Molecular Weight: 718.635

Synonyms:1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide

Chemical Property of 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide

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Technology Process of 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide

There total 4 articles about 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

1-(phenyl-2-ethyl)-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridine (134200-08-1) + methyl iodide (74-88-4) → 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide (134172-74-0)

Guidance literature:

In acetonitrile; for 192h; Heating;

DOI:10.1016/S0040-4020(01)90500-9

Reference yield:

L-Phenylalaninol (3182-95-4) → 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide (134172-74-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 12 h / Ambient temperature

2: 56 percent / acetonitrile / 192 h / Heating

With triethylamine; In dichloromethane; acetonitrile;

DOI:10.1016/S0040-4020(01)90500-9

Reference yield:

1-Phenethyl-1H-pyrrolo[2,3-b]pyridine-3,5-dicarbonyl dichloride → 1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridinium iodide (134172-74-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 12 h / Ambient temperature

2: 56 percent / acetonitrile / 192 h / Heating

With triethylamine; In dichloromethane; acetonitrile;

DOI:10.1016/S0040-4020(01)90500-9

upstream raw materials:

1-(phenyl-2-ethyl)-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-pyrrolo<2,3-b>pyridine

methyl iodide

L-Phenylalaninol

1-Phenethyl-1H-pyrrolo[2,3-b]pyridine-3,5-dicarboxylic acid

Downstream raw materials:

1-(phenyl-2-ethyl)-7-methyl-3,5-N,N-bis-<(S)-(1-benzylhydroxyethyl)aminocarbonyl>-4,7-dihydropyrrolo<2,3-b>pyridine

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