tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate

Base Information

• Chemical Name: tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate
• CAS No.: 535960-11-3
• Molecular Formula: C₅₂H₅₄N₄O₆
• Molecular Weight: 831.024
• Mol file: 535960-11-3.mol

Synonyms:tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate

Chemical Property of tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate

There total 2 articles about tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + - → tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate (535960-11-3)

Guidance literature:

With dmap; In tetrahydrofuran; for 24h; Heating;

DOI:10.1021/ma030033+

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + N-(diphenylmethylene)-N'-(tert-butoxycarbonyl)-N'-(4-bromophenyl)-p-phenylenediamine (200395-28-4) + N′-(tert-butoxycarbonyl)-N′-(phenyl)-p-phenylenediamine (409357-04-6) → tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate (535960-11-3)

Guidance literature:

N-(diphenylmethylene)-N'-(tert-butoxycarbonyl)-N'-(4-bromophenyl)-p-phenylenediamine; N′-(tert-butoxycarbonyl)-N′-(phenyl)-p-phenylenediamine; With palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In tetrahydrofuran; for 24h; Inert atmosphere; Reflux;

di-tert-butyl dicarbonate; With dmap; In tetrahydrofuran; for 24h; Reflux;

DOI:10.1039/b820392j

Reference yield:

tert-butyl (4-((tert-butoxycarbonyl)(4-((tert-butoxycarbonyl)(4-((diphenylmethylene)amino)phenyl)amino)phenyl)amino)phenyl)(phenyl)carbamate (535960-11-3) → tert-butyl (4-aminophenyl)(4-((tert-butoxycarbonyl)(4-((tertbutoxycarbonyl)(phenyl)amino)phenyl)amino)phenyl)carbamate (535960-12-4)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In tetrahydrofuran; methanol; for 24h; Heating;

DOI:10.1021/ma030033+

upstream raw materials:

di-tert-butyl dicarbonate

N-(diphenylmethylene)-N'-(tert-butoxycarbonyl)-N'-(4-bromophenyl)-p-phenylenediamine

N′-(tert-butoxycarbonyl)-N′-(phenyl)-p-phenylenediamine

Downstream raw materials:

tert-butyl (4-aminophenyl)(4-((tert-butoxycarbonyl)(4-((tertbutoxycarbonyl)(phenyl)amino)phenyl)amino)phenyl)carbamate