ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate

Base Information

• Chemical Name: ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate
• CAS No.: 444901-25-1
• Molecular Formula: C₁₇H₁₃ClF₃N₃O₆
• Molecular Weight: 447.755
• Mol file: 444901-25-1.mol

Synonyms:ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate

Chemical Property of ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate

There total 1 articles about ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

1-chloro-2,4-dinitro-6-trifluoromethylbenzene (392-95-0) + ethyl (4-chlorobenzyl)carbamate (51172-60-2) → ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate (444901-25-1)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 3h; Heating / reflux;

Reference yield:

ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate (444901-25-1) → ethyl 4-chlorobenzyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamate (444901-26-2)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 7h;

upstream raw materials:

1-chloro-2,4-dinitro-6-trifluoromethylbenzene

ethyl (4-chlorobenzyl)carbamate

Downstream raw materials:

ethyl 4-chlorobenzyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamate