C₁₇H₁₆ClNO

Base Information

Chemical Name:C₁₇H₁₆ClNO
CAS No.:1477476-44-0
Molecular Formula:C₁₇H₁₆ClNO
Molecular Weight:285.773
Hs Code.:

Synonyms:C₁₇H₁₆ClNO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₆ClNO

Chemical Property:

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Technology Process of C₁₇H₁₆ClNO

There total 2 articles about C₁₇H₁₆ClNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-02-5
3'-Chloroacetophenone

: 1477476-44-0
C₁₇H₁₆ClNO

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl acetamide; toluene / 7 h / Reflux

2: sodium iodide; cerium(III) chloride heptahydrate; ammonium acetate / isopropyl alcohol / 4 h / Reflux

With cerium(III) chloride heptahydrate; ammonium acetate; sodium iodide; In N,N-dimethyl acetamide; isopropyl alcohol; toluene;
DOI:10.1039/c3ra41312h

Reference yield:

: 75175-79-0
1-(3-chlorophenyl)-3-dimethylamino-prop-2-en-1-one

: 126-81-8
dimedone

: 1477476-44-0
C₁₇H₁₆ClNO

Guidance literature:: With cerium(III) chloride heptahydrate; ammonium acetate; sodium iodide; In isopropyl alcohol; for 4h; Reflux;
DOI:10.1039/c3ra41312h

Reference yield: 74.0%

: 1477476-44-0
C₁₇H₁₆ClNO

: 108-24-7
acetic anhydride

: 1477476-11-1
4-chloro-2-(7,7-dimethyl-5-oxo-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

Guidance literature:: With [bis(acetoxy)iodo]benzene; palladium diacetate; In acetonitrile; at 100 ℃; for 6h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c3ra41312h