Technology Process of C35H23N3
There total 5 articles about C35H23N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,3-dimethyl-2-imidazolidinone; copper; potassium carbonate;
at 200 ℃;
for 96h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / diethyl ether / 16 h / 20 °C / Inert atmosphere
2: palladium on activated charcoal / toluene / 3 h / 111 °C
3: acetic acid / 8 h / 118 °C / Inert atmosphere
4: potassium carbonate; copper / Tetraethylene glycol dimethyl ether / 24 h / 190 °C / Inert atmosphere
5: potassium carbonate; 1,3-dimethyl-2-imidazolidinone; copper / 96 h / 200 °C / Inert atmosphere
With
1,3-dimethyl-2-imidazolidinone; hydrogenchloride; copper; potassium carbonate; acetic acid;
palladium on activated charcoal;
In
diethyl ether; Tetraethylene glycol dimethyl ether; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium on activated charcoal / toluene / 3 h / 111 °C
2: acetic acid / 8 h / 118 °C / Inert atmosphere
3: potassium carbonate; copper / Tetraethylene glycol dimethyl ether / 24 h / 190 °C / Inert atmosphere
4: potassium carbonate; 1,3-dimethyl-2-imidazolidinone; copper / 96 h / 200 °C / Inert atmosphere
With
1,3-dimethyl-2-imidazolidinone; copper; potassium carbonate; acetic acid;
palladium on activated charcoal;
In
Tetraethylene glycol dimethyl ether; toluene;