(2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine

Base Information

• Chemical Name: (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine
• CAS No.: 114325-69-8
• Molecular Formula: C₁₈H₁₆BrNO
• Molecular Weight: 342.235

Synonyms:(2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine

Chemical Property of (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine

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Technology Process of (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine

There total 3 articles about (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-carboxybenzene diazonium chloride (4661-46-5) + (2-Bromo-phenyl)-furan-2-ylmethyl-methyl-amine (114325-54-1) → (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.02,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine (114325-69-8)

Guidance literature:

With methyloxirane; In 1,2-dichloro-ethane; for 1.5h; Heating;

DOI:10.1021/jo00282a022

Reference yield: 65.0%

(2-Bromo-phenyl)-furan-2-ylmethyl-methyl-amine (114325-54-1) → (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.02,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine (114325-69-8)

Guidance literature:

DOI:10.1021/jo00245a060

Reference yield:

2-bromo-N-methylaniline (6832-87-7) → (2-Bromo-phenyl)-methyl-(11-oxa-tricyclo[6.2.1.02,7]undeca-2,4,6,9-tetraen-1-ylmethyl)-amine (114325-69-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) ether, reflux, 1 h, 2.) reflux, 15 h

2: 65 percent / propylene oxide / 1,2-dichloro-ethane / 1.5 h / Heating

With sodium hydride; methyloxirane; In 1,2-dichloro-ethane;

DOI:10.1021/jo00282a022

upstream raw materials:

2-carboxybenzene diazonium chloride

(2-Bromo-phenyl)-furan-2-ylmethyl-methyl-amine

2-bromo-N-methylaniline

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