4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

Base Information

Chemical Name:4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile
CAS No.:1469868-38-9
Molecular Formula:C₁₈H₉Cl₃N₆O
Molecular Weight:431.668
Hs Code.:

Synonyms:4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

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Chemical Property of 4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

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Technology Process of 4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

There total 3 articles about 4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-((5-chloro-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)amino)benzonitrile

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 1469868-38-9
4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 150 ℃;
DOI:10.1016/j.ejmech.2014.07.104

Reference yield:

: 78706-26-0
5,7-Dichlor-1,2,4-triazolo<1,5-a>pyrimidin

: 1469868-38-9
4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 150 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.07.104

Reference yield:

: 40775-75-5
[1,2,4]triazolo[1,5-a]pyrimidine-5,7-diol

: 1469868-38-9
4-(5-(2,4,6-trichlorophenoxy)-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl)aminobenzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 12 h / 95 °C

2: ethanol / 6 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 150 °C

With potassium carbonate; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.07.104