dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

Base Information

Chemical Name:dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)
CAS No.:1018961-52-8
Molecular Formula:C₃₀H₃₀ClO₂PW
Molecular Weight:672.844
Hs Code.:

Synonyms:dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

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Chemical Property of dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

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Technology Process of dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

There total 1 articles about dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 89916-32-5
chloro(tricarbonyl)(η5-pentamethylcyclopentadienyl)tungsten(II)

: 603-35-0
triphenylphosphine

: 1018961-52-8
dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

Guidance literature:: In benzene; Irradiation (UV/VIS); Ar, equimol., irradiated (UV) for 5 d; solvent removed (vac.), residue washed (hexane), dried (vac.); elem. anal.;
DOI:10.1002/ejic.200700292

Reference yield: 93.0%

: 1018961-52-8
dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

: 1018961-37-9
sodium dicarbonyl(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungstate

Guidance literature:: With sodium amalgam; In tetrahydrofuran; byproducts: NaCl; Ar, Na:W=2:1 molar ratio, stirred for 18 h at ambient temp.; amalgam separated, solvent removed (vac.), ppt. washed (hexane), dried (vac.); elem. anal.;
DOI:10.1002/ejic.200700292

Reference yield: 51.0%

: 1018961-52-8
dicarbonyl(chloro)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

: 753-73-1
dimethyltin dichloride

: dicarbonyl(chlorodimethylstannyl)(η5-pentamethylcyclopentadienyl)(triphenylphosphanyl)tungsten(II)

: Sn(CH₃)2[W(P(C₆H₅)3)(C₅(CH₃)5)(CO)2]2

Guidance literature:: In diethyl ether; byproducts: NaCl; Ar, equimol., stirred at ambient temp. for 16 h; filtered (celite), evapd. to dryness, dissolved (hexane), ppt. (W2 compd.) filtered, dried (vac.), filtrate concd., crystd. at -30°C, solid dried (vac.); elem. anal.;
DOI:10.1002/ejic.200700292