4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

Base Information

Chemical Name:4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate
CAS No.:1383050-92-7
Molecular Formula:C₃₅H₃₆ClN₃O₃
Molecular Weight:582.142
Hs Code.:

Synonyms:4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

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Chemical Property of 4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

Chemical Property:

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Technology Process of 4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

There total 4 articles about 4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383050-91-6
5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridine

: 119441-98-4
2,2-dimethylpropionic 4-chlorobutyl ester

: 1383050-93-8
C₃₅H₃₆ClN₃O₃

: 1383050-92-7
4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

Guidance literature:: With caesium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

Reference yield:

: 40851-95-4
6-chloropyridine-2,3-diamine

: 1383050-93-8
C₃₅H₃₆ClN₃O₃

: 1383050-92-7
4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4 h / 150 °C

1.2: 60 °C

2.1: triethylamine / dichloromethane / 1.5 h / 25 °C

3.1: potassium iodide; caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

With caesium carbonate; triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 27048-04-0
2-amino-6-chloro-3-nitropyridine

: 1383050-93-8
C₃₅H₃₆ClN₃O₃

: 1383050-92-7
4-(5-chloro-2-(trityloxymethyl)-1H-imidazo[4,5-b]pyridin-1-yl)butyl pivalate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tin(II) chloride dihdyrate / ethyl acetate; tert-butyl alcohol / 1 h / 60 °C

1.2: 3 h / 60 °C

2.1: 4 h / 150 °C

2.2: 60 °C

3.1: triethylamine / dichloromethane / 1.5 h / 25 °C

4.1: potassium iodide; caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

With tin(II) chloride dihdyrate; caesium carbonate; triethylamine; potassium iodide; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;