(E)-(methylthio)methyl cinnamate

Base Information

• Chemical Name: (E)-(methylthio)methyl cinnamate
• CAS No.: 99838-00-3
• Molecular Formula: C₁₁H₁₂O₂S
• Molecular Weight: 208.281

Synonyms:(E)-(methylthio)methyl cinnamate

Chemical Property of (E)-(methylthio)methyl cinnamate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (E)-(methylthio)methyl cinnamate

There total 12 articles about (E)-(methylthio)methyl cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(E)-3-phenylacrylic acid (140-10-3) + dimethyl sulfoxide (67-68-5,8070-53-9) → (E)-(methylthio)methyl cinnamate (99838-00-3)

Guidance literature:

With oxalyl dichloride; triethylamine; In dichloromethane; at -60 - 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2007.02.036

Reference yield: 95.0%

dimethyl sulfoxide (67-68-5,8070-53-9) + Cinnamic acid (621-82-9) → (methylthio)methyl cinnamate (99838-00-3,67024-78-6)

Guidance literature:

With t-butyl bromide; sodium hydrogencarbonate; at 25 - 30 ℃; for 24h;

DOI:10.1039/P19810002737

Reference yield: 95.0%

chloro-methylsulfanyl-methane (2373-51-5) + (E)-3-phenylacrylic acid (140-10-3) → (E)-(methylthio)methyl cinnamate (99838-00-3)

Guidance literature:

With N(Et)4⁽¹⁺⁾*(2-pyrrolidone-anion); In N,N-dimethyl-formamide; for 1h; Ambient temperature;

DOI:10.1021/jo00354a030

upstream raw materials:

dimethyl sulfoxide

Cinnamic acid

chloro-methylsulfanyl-methane

(E)-3-phenylacrylic acid

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