Technology Process of C33H38N2O6
There total 7 articles about C33H38N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
periodic acid;
In
tetrahydrofuran;
at 20 ℃;
for 0.0833333h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 0.17 h / 0 °C
2.1: magnesium sulfate / dichloromethane / 1 h / 20 °C
3.1: dichloromethane / -78 - 20 °C / Inert atmosphere
3.2: Reflux
4.1: ethyl acetate; water / 1 h / 20 °C
5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol / 24 h / 20 °C
6.1: periodic acid / tetrahydrofuran / 0.08 h / 20 °C
With
osmium(VIII) oxide; lithium aluminium tetrahydride; magnesium sulfate; 4-methylmorpholine N-oxide; periodic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane; N,N-dimethyl-formamide / 20 °C
2.1: lithium aluminium tetrahydride / diethyl ether / 0.17 h / 0 °C
3.1: magnesium sulfate / dichloromethane / 1 h / 20 °C
4.1: dichloromethane / -78 - 20 °C / Inert atmosphere
4.2: Reflux
5.1: ethyl acetate; water / 1 h / 20 °C
6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol / 24 h / 20 °C
7.1: periodic acid / tetrahydrofuran / 0.08 h / 20 °C
With
osmium(VIII) oxide; lithium aluminium tetrahydride; magnesium sulfate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 4-methylmorpholine N-oxide; periodic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;