2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

Base Information

Chemical Name:2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside
CAS No.:210423-90-8
Molecular Formula:C₂₁H₂₈N₂O₉
Molecular Weight:452.461
Hs Code.:

Synonyms:2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

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Chemical Property of 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

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Technology Process of 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

There total 5 articles about 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 158979-46-5
nitrobenzyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 210423-90-8
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1007/BF02254805

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 210423-90-8
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / HgI₂, 3 Angstroem molecular sieves / 1,2-dichloro-ethane

2: 63 percent / H₂ / Pd/C / tetrahydrofuran / 4 h / Ambient temperature

With 3 A molecular sieve; hydrogen; mercury(II) iodide; palladium on activated charcoal; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1007/BF02254805

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 210423-90-8
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-[p-(n-decanamido)benzyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) D-camphor-10-sulfonic acid, 2.) Et₃N / 1.) dichloroethane, 80 deg C, 2 h

2: ammonium formate / 10percent Pd-C / methanol / 0.08 h / Ambient temperature

With camphor-10-sulfonic acid; ammonium formate; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1016/S0008-6215(97)10051-9