4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

Base Information

Chemical Name:4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate
CAS No.:1338729-03-5
Molecular Formula:CF₃O₃S*C₄₁H₅₃BrN₅
Molecular Weight:844.88
Hs Code.:

Synonyms:4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

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Chemical Property of 4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

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Technology Process of 4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

There total 7 articles about 4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 235095-05-3
1-azido-6-bromohexane

: 1338729-03-5
4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 18 h / 20 °C

3.1: chloroform-d1 / 20 °C

4.1: methanol / 0.67 h / 20 °C

With methanol; n-butyllithium; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; chloroform-d1; hexane; water; tert-butyl alcohol;
DOI:10.1021/ol202516c

Reference yield:

: 956972-12-6
1,3-bis(2,6-diiopropylphenyl)imidazol-2-ylidene borane

: 1338729-03-5
4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 18 h / 20 °C

3.1: chloroform-d1 / 20 °C

4.1: methanol / 0.67 h / 20 °C

With methanol; n-butyllithium; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; chloroform-d1; hexane; water; tert-butyl alcohol;
DOI:10.1021/ol202516c

Reference yield:

: 1338728-76-9
4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene borane

: 1338729-03-5
4-(6-(4-(4-bromophenyl)-1,2,3-triazol-1-yl)hexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium triflate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 18 h / 20 °C

2: chloroform-d1 / 20 °C

3: methanol / 0.67 h / 20 °C

With methanol; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In chloroform-d1; water; tert-butyl alcohol;
DOI:10.1021/ol202516c