[([(4-t-Bu-C₆H₄)NC₆H₄]3N)Cr(III)-THF]

Base Information

• Chemical Name: [([(4-t-Bu-C₆H₄)NC₆H₄]3N)Cr(III)-THF]
• CAS No.: 1080657-98-2
• Molecular Formula: C₅₂H₅₉CrN₄O
• Molecular Weight: 808.063
• Mol file: 1080657-98-2.mol

Synonyms:[([(4-t-Bu-C₆H₄)NC₆H₄]3N)Cr(III)-THF]

Chemical Property of [([(4-t-Bu-C₆H₄)NC₆H₄]3N)Cr(III)-THF]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [([(4-t-Bu-C₆H₄)NC₆H₄]3N)Cr(III)-THF]

There total 1 articles about [([(4-t-Bu-C₆H₄)NC₆H₄]3N)Cr(III)-THF] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + hexane (110-54-3) + [(4-t-Bu-C6H4)NHC6H4]3N (1007603-24-8) + chromium(III) chloride (10025-73-7,16284-59-6) → [([(4-t-Bu-C6H4)NC6H4]3N)Cr(III)-THF] (1080657-98-2) + (CrCl(N(C6H4NC6H4C(CH3)3)3)(OC4H8))*0.75C6H14

Guidance literature:

With KH; In tetrahydrofuran; under inert atm. to soln. ligand in THF KH was added and stirred overnight, CrCl3 was added and stirred overnight; soln. was evapd. in vacuo, residue was extd. with hexane and Et2O, Et2O extract was allowed to stand at room temp.; elem. anal.;

DOI:10.1021/ic801219u

upstream raw materials:

tetrahydrofuran

hexane

[(4-t-Bu-C₆H₄)NHC₆H₄]3N

chromium(III) chloride