6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

Base Information

Chemical Name:6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone
CAS No.:103286-17-5
Molecular Formula:C₁₇H₁₄N₂O₃
Molecular Weight:294.31
Hs Code.:

Synonyms:6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

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Technology Process of 6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

There total 4 articles about 6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 64-17-5
ethanol

: 103286-12-0
6-carboxy-2-phenyl-1(2H)-phthalazinone

: 103286-17-5
6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

Guidance literature:: With thionyl chloride; for 5h; Heating;
DOI:10.1248/cpb.33.2809

Reference yield:

: 2142-73-6
1-(2,5-dimethylphenyl)-1-ethanone

: 103286-17-5
6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

Guidance literature:: Multi-step reaction with 4 steps

1: KMnO₄, K₂CO₃ / H₂O / 2 h / 70 °C

2: aq. HCl / Heating

3: H₂O / 15 h / Ambient temperature

4: 70 percent / SOCl₂ / 5 h / Heating

With hydrogenchloride; potassium permanganate; thionyl chloride; potassium carbonate; In water;
DOI:10.1248/cpb.33.2809

Reference yield:

: 1-oxo-1,3-dihydro-3-hydroxy-2-benzofuran-5-carboxylic acid

: 103286-17-5
6-ethoxycarbonyl-2-phenyl-1(2H)-phthalazinone

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / 15 h / Ambient temperature

2: 70 percent / SOCl₂ / 5 h / Heating

With thionyl chloride; In water;
DOI:10.1248/cpb.33.2809