Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

Base Information

Chemical Name:Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate
CAS No.:108071-96-1
Molecular Formula:C₂₂H₃₃NO₇
Molecular Weight:423.507
Hs Code.:

Synonyms:Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

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Chemical Property of Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

Chemical Property:

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Technology Process of Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

There total 6 articles about Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89278-34-2
8-Benzyloxy-6(S),7(S)-O-isopropylidene-1-octanal

: 108071-96-1
Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

Guidance literature:: Multi-step reaction with 4 steps

1: KO-tBu / CH₂Cl₂ / 0.5 h / -70 °C

2: H₂ / +BF₄- / ethanol / 72 h / 2250.2 Torr / Ambient temperature

3: H₂ / Pd / methanol / 24 h / 2250.2 Torr / Ambient temperature

With potassium tert-butylate; hydrogen; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; palladium; In methanol; ethanol; dichloromethane;

Reference yield:

: 89278-30-8,89361-29-5
(E/Z)-8-Benzyloxy-6(S),7(S)-O-isopropylidene-4-octenal

: 108071-96-1
Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / KO-tBu / CH₂Cl₂ / 0.5 h / -70 °C

2: H₂ / +BF₄- / ethanol / 72 h / 2250.2 Torr / Ambient temperature

3: H₂ / Pd / methanol / 24 h / 2250.2 Torr / Ambient temperature

With potassium tert-butylate; hydrogen; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; palladium; In methanol; ethanol; dichloromethane;

Reference yield:

: 78513-04-9
(4S,5S)-p-toluolsulfonsaeure<(5-benzyloxymethyl-5-hydroxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>ester

: 108071-96-1
Methyl 2(S)-benzyloxycarbonylamino-10-hydroxy-8(S),9(S)-O-isopropylidenedecanoate

Guidance literature:: Multi-step reaction with 5 steps

2: KO-tBu / CH₂Cl₂ / 0.5 h / -70 °C

3: H₂ / +BF₄- / ethanol / 72 h / 2250.2 Torr / Ambient temperature

4: H₂ / Pd / methanol / 24 h / 2250.2 Torr / Ambient temperature

With potassium tert-butylate; hydrogen; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; palladium; In methanol; ethanol; dichloromethane;