3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

Base Information

Chemical Name:3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester
CAS No.:267405-89-0
Molecular Formula:C₁₅H₁₆N₂O₅
Molecular Weight:304.302
Hs Code.:

Synonyms:3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

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Chemical Property of 3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

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Technology Process of 3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

There total 6 articles about 3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 36239-09-5
ethyl chlorocarbonylacetate

: 198821-79-3
3-methoxy-4-(1,3-oxazol-5-yl)aniline

: 267405-89-0
3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/S0960-894X(02)00132-4

Reference yield:

: 13120-77-9
2-methyl-5-nitroanisole

: 267405-89-0
3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / HOAc; conc. H₂SO₄; CrO₃ / 0 - 10 °C

2: 91 percent / conc. HCl / dioxane / Heating

3: 84 percent / K₂CO₃ / methanol / Heating

4: 95 percent / H₂ / Pd/C / 2068.59 Torr

5: 100 percent / Et₃N / CH₂Cl₂

With chromium(VI) oxide; hydrogenchloride; sulfuric acid; hydrogen; potassium carbonate; acetic acid; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1016/S0960-894X(02)00132-4

Reference yield:

: 136507-15-8
4-nitro-2-methoxybenzaldehyde

: 267405-89-0
3-[[3-Methoxy-4-(5-oxazolyl)phenyl]amino]-3-oxopropanoic Acid Ethyl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / K₂CO₃ / methanol / Heating

2: 95 percent / H₂ / Pd/C / 2068.59 Torr

3: 100 percent / Et₃N / CH₂Cl₂

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0960-894X(02)00132-4