TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2

Base Information

Chemical Name:TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2
CAS No.:866563-79-3
Molecular Formula:C₅₈H₇₈Cl₂N₂O₂P₂Si₂Ti
Molecular Weight:1072.17
Hs Code.:

TiCl<sub>2</sub>(C<sub>6</sub>H<sub>2</sub>(O)(C(CH<sub>3</sub>)3)2(P(C<sub>6</sub>H<sub>5</sub>)2NSi(CH<sub>3</sub>)3))2

Synonyms:TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2

Suppliers and Price of TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2

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Chemical Property of TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2

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Technology Process of TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2

There total 1 articles about TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 866563-77-1
C₆H₂(OH)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3)

: 7550-45-0
titanium tetrachloride

: 866563-79-3
TiCl₂(C₆H₂(O)(C(CH₃)3)2(P(C₆H₅)2NSi(CH₃)3))2

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; diethyl ether; under Ar atm. using Schlenk techniques; soln. of n-BuLi added dropwise to soln. of ligand in THF at -78°C; mixt. warmed to room temp.; stirred for 3 h; resulting soln. added to soln. of TiCl4 in Et2O at 78°C; mixt. stirred for 15 h at room; solvent removed (vac.); CH2Cl2 added; stirred for 30 min; filtered; filtrate concd. (vac.); hexane added; cooled slowly to -20°C; elem. anal.;
DOI:10.1016/j.jorganchem.2005.05.028