(+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle

Base Information

Chemical Name:(+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle
CAS No.:121416-53-3
Molecular Formula:C₁₆H₁₆O₂S
Molecular Weight:272.368
Hs Code.:

Synonyms:(+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle

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Chemical Property of (+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle

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Technology Process of (+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle

There total 3 articles about (+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 108341-44-2
(+)-(R)_S-p-tolylsulfinyl-3 (1S,2R,3S,4R) bicyclo(2.2.1)heptene-5 carboxylate de methyle-2

: 121416-53-3
(+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle

Guidance literature:: With 2,4,6-trimethyl-pyridine; acetic anhydride; trifluoroacetic anhydride; 3-4 deg C, 30 min then 35 deg C, 24 h; repeated addition of reagents;

Reference yield: 74.0%

: 108341-38-4
(+)-(R)_S-p-tolylsulfinyl-3 (1S,2S,3R,4R) bicyclo(2.2.1)heptene-5 carboxylate de methyle-2

: 121416-53-3
(+)-p-tolylthio-3 (1S,4R) bicyclo<2.2.1> heptadiene-2,5 carboxylate-2 de methyle

Guidance literature:: With 2,4,6-trimethyl-pyridine; acetic anhydride; trifluoroacetic anhydride; 3-4 deg C, 30 min then 35 deg C, 108 h; repeated addition of reagents;