C₄₉H₆₃N₂O₈P

Base Information

Chemical Name:C₄₉H₆₃N₂O₈P
CAS No.:1037807-56-9
Molecular Formula:C₄₉H₆₃N₂O₈P
Molecular Weight:839.022
Hs Code.:

C<sub>49</sub>H<sub>63</sub>N<sub>2</sub>O<sub>8</sub>P

Synonyms:C₄₉H₆₃N₂O₈P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₆₃N₂O₈P

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Technology Process of C₄₉H₆₃N₂O₈P

There total 6 articles about C₄₉H₆₃N₂O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1037807-54-7
C₄₀H₄₆O₇

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 1037807-56-9
C₄₉H₆₃N₂O₈P

Guidance literature:: With N,N-diisopropylamine tetrazolide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.200702682

Reference yield:

: 1037807-54-7
C₄₀H₄₆O₇

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1037807-56-9
C₄₉H₆₃N₂O₈P

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/cbic.201500436

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 1037807-56-9
C₄₉H₆₃N₂O₈P

Guidance literature:: Multi-step reaction with 5 steps

1: palladium diacetate; triphenylphosphine; triethylamine / acetonitrile / 24 h / Reflux

2: hydrogen; palladium 10% on activated carbon / methanol / 16 h / 20 °C / 2068.65 Torr

3: pyridine / tetrahydrofuran / 3 h / 0 - 20 °C

4: pyridine / 16 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With pyridine; palladium 10% on activated carbon; hydrogen; palladium diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 1: |Heck Reaction;
DOI:10.1002/cbic.201500436