2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

Base Information

Chemical Name:2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole
CAS No.:115420-82-1
Molecular Formula:C₃₂H₂₄NOP
Molecular Weight:469.522
Hs Code.:

2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ<sup>5</sup>-oxazaphosphole

Synonyms:2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

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Chemical Property of 2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

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Technology Process of 2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

There total 5 articles about 2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 3942-85-6
10-imino-10H-phenanthren-9-one

: 603-35-0
triphenylphosphine

: 115420-82-1
2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

Guidance literature:: In acetonitrile; for 2h; Temperature; Schlenk technique; Inert atmosphere; Reflux;
DOI:10.1039/d1nj00660f

Reference yield: 55.0%

: 84-11-7
9,10-phenanthrenequinone

: 603-35-0
triphenylphosphine

: 115420-82-1
2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

Guidance literature:: With ammonia; In pyridine; at 80 - 90 ℃; for 3h;

Reference yield:

: 85-01-8
phenanthrene

: 115420-82-1
2,3-dihydro-2,2,2-triphenylphenanthro<9,10-d>-1,3,2λ⁵-oxazaphosphole

Guidance literature:: Multi-step reaction with 3 steps

1: chromium(VI) oxide

2: ammonia / chloroform; ethanol / 2 h / Reflux

3: acetonitrile / 2 h / Schlenk technique; Inert atmosphere; Reflux

With chromium(VI) oxide; ammonia; In ethanol; chloroform; acetonitrile;
DOI:10.1039/d1nj00660f