5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide

Base Information

• Chemical Name: 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide
• CAS No.: 813463-09-1
• Molecular Formula: C₉H₇N₅O₄S₄
• Molecular Weight: 377.45

Synonyms:5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide

Chemical Property of 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide

Chemical Property:

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Technology Process of 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide

There total 1 articles about 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophosgene (463-71-8) + aminobenzolamide (3523-95-3) → 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide (813463-09-1)

Guidance literature:

With hydrogenchloride;

DOI:10.1016/j.bmcl.2004.09.062

Reference yield: 52.0%

C10H23BN2O2 + 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide (813463-09-1) → Nε-[(4-(5-sulfamoyl-[1,3,4]thiadiazol-2-ylsulfamoyl)-phenyl)thioureido]-L-lysinatodiethylboron

Guidance literature:

In acetone; Reflux;

DOI:10.1016/j.bmcl.2011.03.055

Reference yield:

5-aminofluorescein + 5-(4-isothiocyanato-benzenesulfonylamino)-[1,3,4]thiadiazole-2-sulfonic acid amide (813463-09-1) → [4-(5-sulfamoyl-[1,3,4]thiadiazol-2-ylsulfamoyl)-phenyl]-thioureido-fluorescein

Guidance literature:

In N,N-dimethyl acetamide; at 20 ℃;

DOI:10.1021/jm0501073

upstream raw materials:

thiophosgene

aminobenzolamide

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