2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane

Base Information

• Chemical Name: 2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane
• CAS No.: 149696-67-3
• Molecular Formula: C₂₂H₄₁BN₄P₂
• Molecular Weight: 434.353

Synonyms:2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane

Chemical Property of 2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane

Chemical Property:

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Technology Process of 2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane

There total 1 articles about 2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2,4,6,7-tetra-tert-butyl-3-chloro-3-methyl-2,4,6,7-tetraaza-1,5-diphospha-3-stannabicyclo{3.1.1}heptane + phenylborondichloride (873-51-8) → 2,4,6,7-tetra-tert-butyl-3-phenyl-2,4,6,7-tetraaza-1,5-diphospha-3-borabicyclo{3.1.1}heptane (149696-67-3) + dimethyltin dichloride (753-73-1)

Guidance literature:

In dichloromethane; addn. of C6H5BCl2 in CH2Cl2 to soln. of stannabicycloheptane in CH2Cl2 at -10°C; refluxing for 3 h; removing of solvent in vacuum; heating residue in boiling tolene for 72 h; removing of toluene;; sublimation at 25°C/ 1E-6 Torr with isolation of (CH3)2SnCl2 and at 85°C/ 1E-6 Torr with isolation of borabicycloheptane; contaminated;;

upstream raw materials:

phenylborondichloride

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